反応 #747086

反応方程式

(4Z)-3-amino-4-[(4-aminophenyl)imino]-2-chloro-6-methylcyclohexa-2,5-dien-1-one

sodium hydrosulphite

→

( 2b )

3-amino-4-[(4-aminophenyl)amino]-2-chloro-6-methylphenol

溶媒

sodium hydroxide

methanol

反応条件

後処理

1. 1
   workup.ADDITIONthe solution is treated

実験手順

10 mg (0.04 mol) of (4Z)-3-amino-4-[(4-aminophenyl)imino]-2-chloro-6-methylcyclohexa-2,5-dien-1-one are added to a solution comprising 16 mg of sodium hydrosulphite in 500 μl of methanol and 5 μl of an aqueous sodium hydroxide solution. The reaction medium is stirred and then the solution is treated according to the usual procedure and characterized. 3-Amino-4-[(4-aminophenyl)amino]-2-chloro-6-methylphenol) (2b) is obtained.

出典