反応 #74686

反応方程式

triphenylphosphine

chloromethyl ethyl ether

→

(Ethoxymethyl)triphenylphosphonium chloride

溶媒

benzene

反応条件

後処理

1. 1
   温度The mixture then was chilled
2. 2
   ろ過filtered
3. 3
   その他to give 7

実験手順

A solution of 99.66 g of triphenylphosphine and 37.82 g of chloromethyl ethyl ether in 240 ml of dry benzene was stirred and refluxed (84° C.) for 6 hours. The mixture then was chilled and filtered to give 7, as a white solid, mp 205°-206° C.

出典