反応 #742271

ord-07047aba1c4045b6a58f03f746e70f9c

反応方程式

CCN(C)C
dimethylethylamine
O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid
CCN(C)C
dimethylethylamine
O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid
→
CC[NH+](C)C.O=S(=O)([O-])C(F)(F)F
Dimethylethylammonium Trifluoromethanesulfonate

反応物

CCN(C)C
dimethylethylamine
O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid
CCN(C)C
dimethylethylamine
O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    温度while being cooled by liquid nitrogen
  2. 2
    その他thus obtaining a target ionic conductor

実験手順

Equimolar amounts of dimethylethylamine and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed dimethylethylamine and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08071253B2uspto-grants-2011_12