反応 #739710

反応方程式

1-[4-(2-bromoethoxy)-3-hydroxy-2-propylphenyl]ethanone

ethyl 2-hydroxybenzoate

potassium carbonate

→

2-[2-(4-acetyl-3-hydroxy-2-propylphenoxy)ethoxy]benzoic acid methyl ester

収率 59.0%

反応条件

後処理

1. 1
   その他to react

実験手順

A mixture of 1.5 g of 1-[4-(2-bromoethoxy)-3-hydroxy-2-propylphenyl]ethanone, 0.76 g of ethyl 2-hydroxybenzoate and 1.05 g of potassium carbonate was allowed to react according to the procedure of Example 79 to give 1.1 g, m.p. 84°-87°, (59% yield) of 2-[2-(4-acetyl-3-hydroxy-2-propylphenoxy)ethoxy]benzoic acid methyl ester, the title compound.

出典