反応 #73546

ord-4bb281048f28408e8885ca421d2baf5d

反応方程式

CC1(C)OCC(CNC2CCCC2)CO1
N-[(2,2-dimethyl-1,3-dioxan-5-yl)methyl]cyclopentanamine
O=S(=O)(Cl)c1ccc(Cl)nc1
6-chloropyridine-3-sulfonyl chloride
NN.O
hydrazine hydrate
→
CC1(C)OCC(CN(C2CCCC2)S(=O)(=O)c2ccc(NN)nc2)CO1
N-cyclopentyl-N-[(2,2-dimethyl-1,3-dioxan-5-yl)methyl]-6-hydrazinylpyridine-3-sulfonamide

反応物

CC1(C)OCC(CNC2CCCC2)CO1
N-[(2,2-dimethyl-1,3-dioxan-5-yl)methyl]cyclopentanamine
O=S(=O)(Cl)c1ccc(Cl)nc1
6-chloropyridine-3-sulfonyl chloride
NN.O
hydrazine hydrate

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他The compound is prepared

実験手順

The compound is prepared according to processes 14.1 and 5.2, starting with N-[(2,2-dimethyl-1,3-dioxan-5-yl)methyl]cyclopentanamine, 6-chloropyridine-3-sulfonyl chloride and hydrazine hydrate.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08541455B2uspto-grants-2013_09