反応 #7318

ord-befbfb3aff7c451d95620ddeb9864f61

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

731 g (2.59 mol) of trifluoromethanesulfonic anhydride and 232 g (2.58 mol) of dimethyl carbonate are added to the residue, and the process described above is repeated. 837 g of methyl trifluoromethanesulfonate having a purity of greater than 99% are isolated (yield: 99.1%).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07084290B2uspto-grants-2006_08