反応 #72625

反応方程式

2-aminobenzonitrile

benzoyl isocyanate

→

N-(2-Cyanophenylcarbamoyl)benzamide

反応条件

実験手順

Prepared as in Example 1a from 2-aminobenzonitrile and benzoyl isocyanate as a white powder (661 mg, 59%). 1H NMR (400 MHz, DMSO-d6) δ7.27-7.29 (t, 1H), 7.52-7.56 (t, 1H), 7.64-7.74 (m, 2H), 7.82-7.85 (dd, 1H), 8.02-8.04 (m, 2H), 8.22-8.24 (d, 1H). MS 266 (MH+).

出典