反応 #725961

反応方程式

p-Cyclohexylphenol

2-chloroethyl vinyl ether

sodium hydroxide

triethylamine

→

4-cyclohexylphenoxyethyl vinyl ether

溶媒

toluene

反応条件

後処理

1. 1
   その他reacted at 120° C. for 5 hours
2. 2
   洗浄The reaction solution was washed with water, excess chloroethyl vinyl ether and toluene
3. 3
   workup.DISTILLATIONwere distilled off
4. 4
   workup.DISTILLATIONthe obtained oil was purified by distillation under reduced pressure

実験手順

p-Cyclohexylphenol (83.1 g (0.5 mol)) was dissolved in 300 ml of toluene and subsequently, 150 g of 2-chloroethyl vinyl ether, 25 g of sodium hydroxide, 5 g of tetrabutylammonium bromide and 60 g of triethylamine were added and reacted at 120° C. for 5 hours. The reaction solution was washed with water, excess chloroethyl vinyl ether and toluene were distilled off, and the obtained oil was purified by distillation under reduced pressure to obtain 4-cyclohexylphenoxyethyl vinyl ether.

出典