反応 #71895

反応方程式

butyl cis(±)-2-(4-{[(benzyloxy)carbonyl]amino}-3-methoxypiperidin-1-yl)-5-methyl-1,3-oxazole-4-carboxylate

→

title compound

収率 113.5%

Butyl cis(±)-2-(4-amino-3-methoxypiperidin-1-yl)-5-methyl-1,3-oxazole-4-carboxylate

収率 113.5%

溶媒

ethyl acetate

反応条件

実験手順

The same operation as in Example (95b) was performed using butyl cis(±)-2-(4-{[(benzyloxy)carbonyl]amino}-3-methoxypiperidin-1-yl)-5-methyl-1,3-oxazole-4-carboxylate obtained in Example (106b) (0.82 g, 1.84 mmol), 10% Pd/C (0.25 g) and ethyl acetate (15 mL), to obtain 0.65 g of the title compound as a yellow amorphous solid (100%).

出典