反応 #71572

反応方程式

tetrahydrothiophene

methyltrifluoromethane sulfonate

→

Methyl-Tetrahydrothiophene Triflate

溶媒

dichloromethane

反応条件

後処理

1. 1
   その他As a result, a white solid product in a salt form was obtained after about 5 minutes
2. 2
   ろ過The solid product was filtered
3. 3
   その他dried for 1 hour in an oven at 50° C.
4. 4
   その他to obtain the following product

実験手順

11 mmol of tetrahydrothiophene was dissolved in 10 ml of dichloromethane at 0° C., and about 12 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture. As a result, a white solid product in a salt form was obtained after about 5 minutes. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:

出典