反応 #71259

ord-a22ec2a4848845ee8dad873524be504d

反応方程式

CCCCCCCCCCCC(=O)OCC(O)CO
glycerol monolaurate
CCCCCCCCCCCCCCCCO
cetyl alcohol
CCCCCCCCCCCC(=O)OCC(O)CO
glycerol monolaurate
CCCCCCCCCCCCCCCCO
cetyl alcohol
CCCCCCCCCCCCCCCCCC(=O)O
stearic acid
CCCCCCCCCC[N+](C)(C)CCCCCCCCCC.[Cl-]
DDAC
CCCCCCCCCCCCCCCCCC(=O)O.OCCN(CCO)CCO
Triethanolamine Stearate

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    workup.ADDITIONInstead of being added in the second step
  2. 2
    workup.ADDITIONwas added
  3. 3
    workup.ADDITIONafter the addition of TEA

実験手順

Example 2A was repeated but for the sequence of addition of glycerol monolaurate and cetyl alcohol. Instead of being added in the second step, after the equimolar mixture of stearic acid and DDAC, the same amount of the glycerol monolaurate and cetyl alcohol added in Example 2 was added after the addition of TEA.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08536228B2uspto-grants-2013_09