反応 #70898

反応方程式

nicotinic acid

POCl3

→

Nicotinoyl chloride hydrochloride

反応条件

後処理

1. 1
   温度at reflux for 1.5 h
2. 2
   濃縮concentrated
3. 3
   その他The product obtained
4. 4
   その他was directly used in the next reaction

実験手順

A solution of nicotinic acid (0.50 g, 4.0 mmol) and POCl3 (5 mL) was heated at reflux for 1.5 h and concentrated. The product obtained was directly used in the next reaction.

出典