反応 #707873

反応方程式

( D2.1 )

Methacrylate

TBAF

Irganox 1010

→

Allyl Methacrylate

溶媒

THF

反応条件

後処理

1. 1
   温度The mixture warmed up
2. 2
   その他The last traces of THF were removed
3. 3
   温度by heating in a vacuum oven at 60° for 4 hours

実験手順

To a stirred solution of MTS (5.5×10-3 g) in dry THF (10.0 ml) was added (D2.1) (3.0 g), AM (0.11 ml) and TBAF (2 μ1 of 1M THF solution). The mixture warmed up and was stirred overnight at room temperature. 50 ppm Irganox 1010 antioxidant was added to the very viscous clear solution, which was cast into a polyester tray in a stream of nitrogen. The last traces of THF were removed by heating in a vacuum oven at 60° for 4 hours.

出典