反応 #707641

ord-81048ea7faf3483092d2da47a242376d

反応方程式

CC(C)C(O)C(C)(C)CO
2,2,4-trimethyl-1,3-dihydroxypentane
O=[N+]([O-])c1ccc(Cl)cc1
4-nitrochlorobenzene
[Na+].[OH-]
sodium hydroxide
CC(C)C(Oc1ccc([N+](=O)[O-])cc1)C(C)(C)COc1ccc([N+](=O)[O-])cc1
1,3-bis-(4-nitrophenoxy)-2,2,4-trimethylpentane

溶媒

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他were reacted

実験手順

146 g (1 mol) 2,2,4-trimethyl-1,3-dihydroxypentane, 346.5 g (2.2 mols) 4-nitrochlorobenzene and 140 g powdered sodium hydroxide were reacted using the same procedure described in Example 1 in 600 ml DMSO.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04820866uspto-grants-1989_04