反応 #70287

反応方程式

3-bromophenol

bromocyclopropane

K2CO3

Water

→

expected product

収率 83.1%

1-Bromo-3-cyclopropoxybenzene

収率 83.1%

溶媒

DMF

diethyl ether

反応条件

後処理

1. 1
   その他the organic phase was evaporated

実験手順

A mixture of 3-bromophenol (4.80 mmol, 0.83 g), bromocyclopropane (27.71 mmol, 2.22 ml), K2CO3 (23.15 mmol, 3.2 g) in DMF (18 ml) was heated at 180° C. for 8 hours in a microwave oven. Water and diethyl ether were added and the organic phase was evaporated affording 0.85 g of the expected product.

出典