反応 #70203

反応方程式

ether

2′-Iodo-5′-isopropoxy-4′-methoxypropiophenone

→

5′-Hydroxy-2′-iodo-4′-methoxypropiophenone

溶媒

ethyl acetate hexane

反応条件

実験手順

Concentration of fraction B (Rf 0.7 in 1:1 v/v ethyl acetate/hexane) afforded the starting ether 11 (98 mg, 21% recovery) as a pale-yellow oil that was identical, as judged by 1H NMR spectroscopic analysis, with authentic material.

出典