反応 #688920

反応方程式

2-methyl-4-oxatricyclo[5.2.1.02,6]-decan-3-ol

acetic anhydride

→

target compound

収率 96.0%

2-methyl-4-oxatricyclo[5.2.1.02,6]decan-3-yl acetate

収率 96.0%

溶媒

pyridine

反応条件

後処理

1. 1
   濃縮The reaction mixture was concentrated
2. 2
   workup.DISTILLATIONThe concentrate was purified by distillation

実験手順

A mixture of 63 g of 2-methyl-4-oxatricyclo[5.2.1.02,6]-decan-3-ol, 42 g of pyridine, and 51 g of acetic anhydride was heated at 50° C. for 5 hours. The reaction mixture was concentrated. The concentrate was purified by distillation, obtaining 74 g (yield 96%) of the target compound.

出典