反応 #68859

反応方程式

6-chloro-2-methyl-quinoline

1,4-dioxane

→

title compound

6-Chloro-quinoline-2-carbaldehyde

反応条件

後処理

1. 1
   ろ過The resulting black mixture was filtered through diatomaceous earth

実験手順

A suspension of 6-chloro-2-methyl-quinoline (355 mg) and SeO2 (233 mg) in 1,4-dioxane (3 mL) was heated at 80° C. for 16 h. The resulting black mixture was filtered through diatomaceous earth. Concentration of the filtrate gave the title compound as a yellow powder (324 mg).

出典