反応 #68781

ord-57cff594de224c42a16d335ca7ca622e

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    濃縮The mixture is concentrated in vacuo

実験手順

1.0 g (6.40 mmol) 2-Amino-oxazole-4-carboxylic acid ethyl ester and 9.1 mL (96.3 mmol) acetic acid anhydride are stirred for 2 d at rt. The mixture is concentrated in vacuo to yield the desired product which is used without further purification.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08530461B2uspto-grants-2013_09