反応 #67854

反応方程式

3-[(2-chloro-4-iodophenyl)amino]isonicotinic acid

intermediate 2

3-[(2-chloro-4-iodophenyl)amino]isonicotinic acid

O-methyl-hydroxylamine

→

N-methoxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide

反応条件

後処理

1. 1
   その他LC/MS [8.75 min; 404 (M+1)]

実験手順

N-methoxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.30 mmol of 3-[(2-chloro-4-iodophenyl)amino]isonicotinic acid (intermediate 2) and 0.42 mmol of O-methyl-hydroxylamine. LC/MS [8.75 min; 404 (M+1)]

出典