反応 #674286

反応方程式

calcium chloride

hydrogen phosphate

NaOH

→

Calcium Phosphate

反応条件

後処理

1. 1
   その他CaP NPs
2. 2
   その他were obtained by filtration of the suspension through a 0.22 μm
3. 3
   ろ過filter
4. 4
   その他CaP NPs
5. 5
   その他were stored at 4° C. before use
6. 6
   その他CaP/ZOL-NPs complexes (CaPZ NPs) were prepared
7. 7
   workup.ADDITIONby mixing a CaP NPs dispersion with an aqueous solution of ZOL
8. 8
   濃縮at different ZOL concentrations (10 mg/ml of ZOL in water or 50 mg/ml of ZOL in phosphate buffer at pH 9.5)

実験手順

An aqueous solution of calcium chloride (18 mM) was added, dropwise and under magnetic stirring, to an aqueous solution on dibasic hydrogen phosphate (10.8 mM). The pH of both solutions was adjusted beforehand to 9.5 with NaOH. CaP NPs were obtained by filtration of the suspension through a 0.22 μm filter. CaP NPs were stored at 4° C. before use. CaP/ZOL-NPs complexes (CaPZ NPs) were prepared by mixing a CaP NPs dispersion with an aqueous solution of ZOL at different ZOL concentrations (10 mg/ml of ZOL in water or 50 mg/ml of ZOL in phosphate buffer at pH 9.5), at a volume ratio of 50:1.

出典