反応 #670490

反応方程式

product

2-[Benzyl-(4-methoxy-benzenesulfonyl)-amino]-3-hydroxy-benzoic acid methyl ester

methyl 4-(bromomethyl)benzoate

→

desired product

収率 87.0%

2-[Benzyl-(4-methoxy-benzenesulfonyl)-amino]-3-(4-methoxycarbonyl-benzyloxy)-benzoic acid methyl ester

収率 87.0%

反応条件

実験手順

In the same manner as described in Example 38, 0.275 g (0.644 mmol) of the product of Example 37 and 0.295 g (1.288 mmol) of methyl 4-(bromomethyl)benzoate provided 0.322 g (87%) of the desired product as a white solid. Electrospray Mass Spec: 576.2 (M+H)+

出典