反応 #6698

反応方程式

7-chlorolepidine

CH3I

diethyl ether

→

7-chloro-1-methyllepidinium iodide

溶媒

CH3CN

反応条件

後処理

1. 1
   温度at reflux for two hours
2. 2
   その他to give a yellow powder

実験手順

A portion of the 7-chlorolepidine (80 mg) prepared as above was methylated by heating with CH3I (0.5 ml) in CH3CN (1 ml) at reflux for two hours. The mixture was treated with diethyl ether, followed by centrifugation, to give a yellow powder.

出典