反応 #6683

反応方程式

[R]-1-trifluoromethylheptyl 4-benzyloxybenzoate

→

[R]-1-Trifluoromethylheptyl 4-hydroxybenzoate

収率 99.0%

溶媒

ethyl acetate

反応条件

後処理

1. 1
   ろ過Then the catalyst was filtered out
2. 2
   その他filtrate was evaporated to dryness
3. 3
   その他to give the pure compound in yield of 99%

実験手順

2.2 g of [R]-1-trifluoromethylheptyl 4-benzyloxybenzoate, (13) 100 mg of PdOH/C in 50 ml of ethyl acetate was stirred at RT over night under H2 atmosphere. Then the catalyst was filtered out and filtrate was evaporated to dryness to give the pure compound in yield of 99%.

出典