反応 #66011
ord-9ce66c0ac6a9497f90fd9e34b54bd9d0
反応方程式
allyloxyethyl sulfate
C8F17I
→
2-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundec-2-enyloxy)ethyl hydrogen sulfate
試薬
なし
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
Crystalline allyloxyethyl sulfate (Na salt) from the preparation shown in example 2 was perfluoroalkylated using the procedure of example 7 and C8F17I to produce 2-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundec-2-enyloxy)ethyl hydrogen sulfate.