反応 #66010

反応方程式

allyl bromide

diethylene glycol

→

Diethylene glycol monoallyl ether

収率 82.0%

溶媒

THF NaH

反応条件

後処理

1. 1
   その他The product was obtained in 82% yield
2. 2
   workup.DISTILLATIONafter distillation

実験手順

Diethylene glycol monoallyl ether was prepared by reacting allyl bromide with excess diethylene glycol in THF-NaH (tetrahydrofuran-sodium hydride). The product was obtained in 82% yield after distillation. b.p.=96-99° C./7 mmHg.

出典