反応 #65962

ord-845bb11cfab64d898e0390f7ee4a116c

反応方程式

Oc1cccc2ccccc12
1-naphthol
C=O
formalin
C1CCNCC1
piperidine
C1COCCN1
morpholine
Oc1c(CN2CCCCC2)ccc2ccccc12
2-(piperidinomethyl)-1-naphthol
Oc1c(CN2CCOCC2)ccc2ccccc12
2-(morpholinomethyl)-1-naphthol

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Anon. (USA) (Res. Discl., 236, 380 (Ger), 1983) discloses a Mannich reaction of 1-naphthol with formalin and piperidine or morpholine to yield 2-(piperidinomethyl)-1-naphthol or 2-(morpholinomethyl)-1-naphthol, respectively. These compounds were subjected to hydrogenolysis (Pd/C) whereby 2-methyl-1-naphthol was produced

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05420362uspto-grants-1995_05