反応 #65709

ord-04d4bd6038684c3585865756f2f86541

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

In analogy to Example 45, by reacting [1-(2,2-dimethyl-1,3-benzodithiol-5-yl)ethyl]triphenylphosphonium bromide with benzaldehyde, there was obtained 2,2-dimethyl-5-[(E)-α-methylstyryl]-1,3-benzodithiol, melting point 57°-58° C.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05420273uspto-grants-1995_05