反応 #651855

ord-cd73f84037244cc6a695c8ccf5276666

反応方程式

CCCCCCCCc1ccc2c(c1)CC(F)c1cc(CCCCCCCC)ccc1-2
9-fluoro-2,7-dioctyl-9,10-dihydrophenanthrene
N#CC1=C(C#N)C(=O)C(Cl)=C(Cl)C1=O
DDQ
→
CCCCCCCCc1ccc2c(c1)cc(F)c1cc(CCCCCCCC)ccc12
9-Fluoro-2,7-dioctylphenanthrene

反応物

CCCCCCCCc1ccc2c(c1)CC(F)c1cc(CCCCCCCC)ccc1-2
9-fluoro-2,7-dioctyl-9,10-dihydrophenanthrene
N#CC1=C(C#N)C(=O)C(Cl)=C(Cl)C1=O
DDQ

試薬

なし

溶媒

Cc1ccccc1
toluene

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

From 9-fluoro-2,7-dioctyl-9,10-dihydrophenanthrene by dehydrogenation with DDQ in toluene.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US06168838Auspto-grants-2001_01