反応 #651854

ord-a519817476894e4b91f9d4d0493d56fd

反応方程式

CCCCCCCCc1ccc2c(c1)CC(O)c1cc(CCCCCCCC)ccc1-2
2,7-dioctyl-9,10-dihydrophenanthren-9-ol
CCN(CC)S(F)(F)F
DAST
→
CCCCCCCCc1ccc2c(c1)CC(F)c1cc(CCCCCCCC)ccc1-2
9-Fluoro-2,7-dioctyl-9,10-dihydrophenanthrene

反応物

CCCCCCCCc1ccc2c(c1)CC(O)c1cc(CCCCCCCC)ccc1-2
2,7-dioctyl-9,10-dihydrophenanthren-9-ol
CCN(CC)S(F)(F)F
DAST

試薬

なし

溶媒

ClCCl
dichloromethane

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

From 2,7-dioctyl-9,10-dihydrophenanthren-9-ol by reaction with DAST in abs. dichloromethane.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US06168838Auspto-grants-2001_01