反応 #65101

反応方程式

4-n-octyloxyterphenyl-4"-carboxylic acid

thionyl chloride

→

4-n-octyloxyterphenyl-4"-carboxylic acid chloride

反応条件

後処理

1. 1
   温度under reflux condition for 6 hours
2. 2
   workup.DISTILLATIONunreacted thionyl chloride was distilled off

実験手順

After 1.6 g of 4-n-octyloxyterphenyl-4"-carboxylic acid was heated with an excess amount of thionyl chloride under reflux condition for 6 hours, unreacted thionyl chloride was distilled off to obtain 4-n-octyloxyterphenyl-4"-carboxylic acid chloride.

出典