反応 #64726
ord-d83f8938d53c49d9bb2e0f29f30c50d5
反応方程式
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他obtained by Reference Example 1
- 2濃縮the reaction mixture was concentrated under reduced pressure
実験手順
In 50 ml of methylene chloride was dissolved 7 g of 2-[bis(4-acetoxyphenyl)methyl]benzoic acid obtained by Reference Example 1, and then 10 ml of thionyl chloride was added dropwise to the solution at room temperature. The reaction mixture was stirred for 2 hours, and the reaction mixture was concentrated under reduced pressure to afford 11.33 g of the desired compound as an oily matter.