反応 #64223

反応方程式

acetone cyanohydrin

4-amino 1-butanol

→

propanonitrile

2-(4-hydroxybutylamino) 2-methylpropano-nitrile

溶媒

methylene chloride

反応条件

後処理

1. 1
   その他dried
2. 2
   ろ過filtered
3. 3
   濃縮the filtrate was concentrated under reduced pressure

実験手順

220 μl of acetone cyanohydrin and 200 μl of 4-amino 1-butanol were mixed together with stirring for 16 hours at 20° C. and then was diluted with 2 ml of methylene chloride, dried, filtered and the filtrate was concentrated under reduced pressure to obtain the propanonitrile which was used as is for the following stage.

出典