反応 #64061

ord-d6a2513d2daa45ca9c05c03ed0d3747b

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

5-(2,6-Dimethyl-4-hydroxyphenyl)-2-[1-(ethoxyimino)propyl]-3-hydroxycyclohex-2-en-1-one (31) was prepared from 5-(2,6-dimethyl-4-hydroxyphenyl)-3-hydroxy-2-propionylcyclohex-2-en-1-one and ethoxyamine hydrochloride following essentially the same procedure as that described in Example 1, part (iv). The product was characterized by proton nuclear magnetic resonance spectroscopy and the spectroscopic data is reported in Table 5, Example 37.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04767879uspto-grants-1988_08