反応 #640563

反応方程式

2-aminophenylboronic acid

acryloyl chloride

→

2-Acrylamido-phenylboronic acid

反応条件

後処理

1. 1
   抽出The product was extracted in acetone
2. 2
   その他dried
3. 3
   その他a rotary evaporator

実験手順

2-Acrylamido-phenylboronic acid (“2-APB”) was synthesized by reacting 2-aminophenylboronic acid with an excess of acryloyl chloride in an aqueous alkaline solution. The product was extracted in acetone and dried using a rotary evaporator. The structure of 2-APB was confirmed using NMR. The purity was shown to be greater than 90%.

出典