反応 #640562

反応方程式

3-amino phenylboronic acid

acryloyl chloride

→

3-Acrylamido-phenylboronic acid

反応条件

後処理

1. 1
   抽出The product was extracted in acetone
2. 2
   その他dried
3. 3
   その他a rotary evaporator

実験手順

3-Acrylamido-phenylboronic acid (“3-APB”) was synthesized by reacting 3-amino phenylboronic acid with an excess of acryloyl chloride in an aqueous alkaline solution. The product was extracted in acetone and dried using a rotary evaporator. The structure of 3-APB was confirmed using NMR. The purity was about 90%, TLC showing very little contamination.

出典