反応 #63447
ord-d86ea385bc984b039dc781fd12477b0e
反応方程式
5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile
cyclohexanol
→
cyclohexyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and cyclohexanol there is obtained cyclohexyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a syrup, 1H-NMR(CDCl3): 1.5-2.1 (8H), 4.2 (s, 4H), 4.67 (broad s, NH), 5.1 (m, OCH), 7.3-7.7 (8H).