反応 #63364

反応方程式

3-ethyl-1-(4-nitrophenyl)-3-azabicyclo[3.1.1-]heptane-2,4-dione

→

1-(4-aminophenyl)-3-ethyl-3-azabicyclo[3.1.1]heptane-2,4-dione

溶媒

methanol

反応条件

実験手順

In a manner analogous to that described in Example 1a, 2.33 g of 3-ethyl-1-(4-nitrophenyl)-3-azabicyclo[3.1.1-]heptane-2,4-dione in 70 ml of methanol are hydrogenated in the presence of 0.15 g of palladium-on-carbon and worked up. Melting point 159°-162° (from ethyl acetate/petroleum ether).

出典