反応 #63312

反応方程式

cyanocarbonimidodithioic acid dimethyl ester

benzaldehyde N-methyl hydrazone

→

title compound

N-Cyano-1-methyl-2-(phenylmethylene)hydrazinecarboximidothioic acid, methyl ester

溶媒

acetonitrile

反応条件

後処理

1. 1
   温度was heated
2. 2
   温度under reflux for 50 hr
3. 3
   温度The reaction mixture was cooled to 25°

実験手順

A mixture of cyanocarbonimidodithioic acid dimethyl ester (1.46 g) and benzaldehyde N-methyl hydrazone (1.34 g) in acetonitrile was heated under reflux for 50 hr. The reaction mixture was cooled to 25° to give the title compound as colourless crystals, m.p. 132°-133° (0.73 g).

出典