反応 #632015

反応方程式

1-methoxymethylcyclopropylsulfonylamine tert-butylcarbamate

3,5-dimethylisoxazole-4-isocyanate

→

1-(3,5-dimethylisoxazol-4-yl)carbamoylcyclopropanesulfonamide tert-butylcarbamate

収率 100.0%

反応条件

後処理

1. 1
   その他This compound was obtained in a crude 100% yield
2. 2
   その他The compound was taken directly into the next reaction without purification

実験手順

This compound was obtained in a crude 100% yield according to the procedure described for the synthesis of 1-methoxymethylcyclopropylsulfonylamine tert-butylcarbamate except that 1.20 equivalents of 3,5-dimethylisoxazole-4-isocyanate was used as the electrophile. The compound was taken directly into the next reaction without purification.

出典