反応 #632009

反応方程式

N-tert-butyl-(1-methyl)cyclopropylsulfonamide

allyl bromide

→

N-tert-butyl-(1-allyl)cyclopropylsulfonamide

収率 97.0%

反応条件

後処理

1. 1
   その他This compound was obtained in 97% yield
2. 2
   その他The compound was used in the next reaction without further purification

実験手順

This compound was obtained in 97% yield according to the procedure described in the synthesis of N-tert-butyl-(1-methyl)cyclopropylsulfonamide using 1.25 equivalents of allyl bromide as the electrophile. The compound was used in the next reaction without further purification: 1H NMR (CDCl3) δ 0.83 (m, 2H), 1.34 (s, 9H), 1.37 (m, 2H), 2.64 (d, J=7.3 Hz, 2H), 4.25 (br s, 1H), 5.07-5.10 (m, 2H), 6.70-6.85 (m, 1H).

出典