反応 #631975

反応方程式

6-hydroxy-2-naphthyl benzoate

nitric acid

water

→

6-hydroxy-5-nitro-2-naphthyl benzoate

溶媒

acetic acid

反応条件

後処理

1. 1
   その他at 15° C.
2. 2
   その他The thus obtained deposit was recrystallized from ethanol/acetic acid

実験手順

The thus obtained 6-hydroxy-2-naphthyl benzoate was dispersed in acetic acid, nitric acid was added dropwise to the dispersion while keeping it at 15° C., and water was further added thereto, followed by stirring. The thus obtained deposit was recrystallized from ethanol/acetic acid to obtain 6-hydroxy-5-nitro-2-naphthyl benzoate.

出典