反応 #631971

反応方程式

2-Carboxyethyl acrylate

Thionyl chloride

→

desired product

3-chloro-3-oxopropyl acrylate

溶媒

CH2Cl2

反応条件

後処理

1. 1
   温度the solution is cooled in an ice bath
2. 2
   その他The solvent is removed under reduced pressure

実験手順

2-Carboxyethyl acrylate (1 eq.) is dissolved in CH2Cl2 and the solution is cooled in an ice bath. Thionyl chloride (1 eq.) is added dropwise and the mixture is allowed to warm to room temperature and stir for 4 hours. The solvent is removed under reduced pressure and the desired product is isolated by vacuum distillation.

出典