反応 #6300
ord-c752070c8b524cd1886a9e0e3e0ee605
反応方程式
4-triflyl-alpha-bromotoluene
triphenylphosphine
→
4-Triflylbenzyltriphenylphosphonium bromide
溶媒
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1温度at reflux for 19 hours
実験手順
A solution of 30.3 g (0.1 mole) of 4-triflyl-alpha-bromotoluene and 28.8 g (0.1 mole) of triphenylphosphine in xylene is heated at reflux for 19 hours. 4-Triflylbenzyltriphenylphosphonium bromide is then isolated by filtration, washed with additional portions of xylene, and dried.