反応 #62970

反応方程式

bromomethyl ethylene glycol

magnesium sulfate

acetone

→

crude product

2,2-Dimethyl-4-bromomethyl-1,3-dioxolane

反応条件

後処理

1. 1
   その他The cooled reaction mixture
2. 2
   ろ過is filtered
3. 3
   その他the solvent is removed

実験手順

An acetone solution of bromomethyl ethylene glycol is refluxed for 24 hours in the presence of anhydrous magnesium sulfate. The cooled reaction mixture is filtered and the solvent is removed to provide a residual crude product.

出典