反応 #62838

ord-e70f97453dcd4210bf2cd121b4ee236a

反応方程式

CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC(=O)O
3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid
OCCNCCO
diethanolamine
→
CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC(=O)N(CCO)CCO
title compound
収率 90.0%
CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC(=O)N(CCO)CCO
N-(3,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenoyl)-diethanolamine
収率 90.0%

反応物

CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC(=O)O
3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid
OCCNCCO
diethanolamine

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

The procedure of Example 1 was repeated except that 6.1 g of 3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid and 2.9 ml of diethanolamine were used as starting materials. 7.0 g (yield 90%) of the title compound was obtained as a colorless oil.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04762829uspto-grants-1988_08