反応 #62820

反応方程式

1-methylcyclohexyl 2-amino-α-methylbenzothiazole-6-acetate

1-adamantyl 2-(p-aminophenyl)propionate

→

1-adamantyl 2-amino-α-methylbenzothiazole-6-acetate

収率 83.0%

反応条件

後処理

1. 1
   その他were reacted

実験手順

Using the methpod similar to that used in the preparation of 1-methylcyclohexyl 2-amino-α-methylbenzothiazole-6-acetate, 19.1 g of 1-adamantyl 2-(p-aminophenyl)propionate were reacted to obtain 18.97 g (83% yield) of 1-adamantyl 2-amino-α-methylbenzothiazole-6-acetate as a creamy white solid melting at 151°-153° C.

出典