反応 #62787

反応方程式

Dichloromaleic anhydride

Bis-(3-chloroallyl)amine

→

above-named product

収率 99.1%

N,N-bis-(3-chloroallyl) dichloromaleic monoamide

収率 99.1%

溶媒

methylene chloride

反応条件

後処理

1. 1
   その他The exothermic reaction
2. 2
   その他yielded a clear solution

実験手順

Dichloromaleic anhydride (1.7 g, 0.01 mol) and 30 ml methylene chloride were stirred under a mild reflux. Bis-(3-chloroallyl)amine (1.7 g, 0.01 mol) was then added. The exothermic reaction yielded a clear solution. The solution was stirred at room temperature for 3 hours. The mixture was stripped, resulting in 3.3 g of the above-named product.

出典