反応 #61847

反応方程式

1-(2-Amino-oxazol-4-yl)-naphthalen-2-ol

1-(2-amino-oxazol-4-yl)-naphthalen-2-ol

sodium hydride

Methyl bromoacetate

→

[1-(2-amino-oxazol-4-yl)-naphthalen-2-yloxy]-acetic acid methyl ester

溶媒

N,N-dimethylformamide

反応条件

後処理

1. 1
   その他to give a dark orange solution

実験手順

1-(2-Amino-oxazol-4-yl)-naphthalen-2-ol (22, 190 mg) was dissolved in N,N-dimethylformamide and then sodium hydride (34 mg) was added in one portion to give a dark orange solution. Methyl bromoacetate (88 μL) was then added and the mixture was stirred at room temperature for 18 hours.

出典