反応 #61447

ord-e0438a7b174843c8a39e6fdf9ab17a95

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他Crystallisation from methanol

実験手順

Prepared in analogy to example 1.18(a) from 2,6-dichloroquinoline and piperazine-1-carboxylic acid tert-butyl ester. Crystallisation from methanol yields the title compound as a colorless solid.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07429585B2uspto-grants-2008_09